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Crystallography A

General data

Course ID: 1200-2EN-CRALE1M
Erasmus code / ISCED: 13.3 Kod klasyfikacyjny przedmiotu składa się z trzech do pięciu cyfr, przy czym trzy pierwsze oznaczają klasyfikację dziedziny wg. Listy kodów dziedzin obowiązującej w programie Socrates/Erasmus, czwarta (dotąd na ogół 0) – ewentualne uszczegółowienie informacji o dyscyplinie, piąta – stopień zaawansowania przedmiotu ustalony na podstawie roku studiów, dla którego przedmiot jest przeznaczony. / (0531) Chemistry The ISCED (International Standard Classification of Education) code has been designed by UNESCO.
Course title: Crystallography A
Name in Polish: Crystallography A
Organizational unit: Faculty of Chemistry
Course groups: (in Polish) Przedmioty obowiązkowe w semestrze 1M (studia w języku angielskim)
ECTS credit allocation (and other scores): 1.00 Basic information on ECTS credits allocation principles:
  • the annual hourly workload of the student’s work required to achieve the expected learning outcomes for a given stage is 1500-1800h, corresponding to 60 ECTS;
  • the student’s weekly hourly workload is 45 h;
  • 1 ECTS point corresponds to 25-30 hours of student work needed to achieve the assumed learning outcomes;
  • weekly student workload necessary to achieve the assumed learning outcomes allows to obtain 1.5 ECTS;
  • work required to pass the course, which has been assigned 3 ECTS, constitutes 10% of the semester student load.

view allocation of credits
Language: English
Type of course:

obligatory courses

Short description:

The basic information about the structure of crystals, symmetry and its properties, properties of X-rays, diffraction theories.

Full description:

The course covers the following issues: Symmetry and its properties, crystallization techniques, crystal growth theories, imperfect crystals, energetic aspects of the crystals structures, classification of solids (ionic, covalent, metallic, molecular) their characteristics. Properties of X-rays. Laue and Bragg’s diffraction theories; reciprocal space. Symmetry of diffraction pattern, Intensity of reflections as a source of information about arrangement of atoms and/or ions in the crystal unit cell. Phase problem. Experimental methods of X-ray crystallography: Laue method, oscillation method, goniometric methods; determination of unit cell parameters; Powder diffraction. Elements of crystallophysics. Interpretation of the crystal and molecular structure based on crystallographic databases

Bibliography:

1. Z. Trzaska Durski, H. Trzaska Durska, Podstawy krystalografii strukturalnej i rentgenowskiej, Wydawnictwo Naukowe PWN, Warszawa, 1994 (in Polish).

2. Z. Bojarski, M. Gigla, K. Stróż, M. Surowiec, Krystalografia. Podręcznik wspomagany komputerowo, Wydawnictwo Naukowe PWN, Warszawa, 1996, 2001, 2007 (in Polish).

3. Z. Trzaska Durski, H. Trzaska Durska, Podstawy krystalografii, Oficyna Wydawnicza Politechniki Warszawskiej, Warszawa 2003 (in Polish).

4. P. Luger, Rentgenografia strukturalna monokryształów, PWN, Warszawa 1989 (in Polish).

5. M. van Meerssche i J. Feneau-Dupont, Krystalografia i chemia strukturalna, PWN, Warszawa 1984 (in Polish).

6. P. Luger, Modern X-ray Analysis on Single Crystals, Walter de Gruyter and Co., Berlin 1980 (in English).

7. C. Giacovazzo, H. Z. Monaco, D. Biterbo, F. Scordari, G. Gilli, G. Zanotti, M. Catti, Fundamentals of Crystallography, IUCR, Oxford University Press, 2000 (in English)

Learning outcomes:

The aim of the course is to present the information that will allow students to use and understand scientific literature on the structures of small molecules determined by X-ray diffraction.

Assessment methods and assessment criteria:

Exam requirements:

- crystallization techniques, crystal growth theories,

- energetic aspects of the crystals structures, classification of solids (ionic, covalent, metallic, molecular)

- Properties of X-rays.

- Laue and Bragg’s diffraction theories;

- reciprocal space.

- Symmetry of diffraction pattern, Intensity of reflections as a source of information about arrangement of atoms and/or ions in the crystal unit cell.

- phase problem and ways to solve it.

- experimental methods of X-ray crystallography: Laue method, oscillation method, goniometric methods; determination of unit cell parameters;

- powder diffraction.

- Elements of crystallophysics.

- Interpretation of the crystal and molecular structure based on crystallographic databases

Practical placement:

none

Classes in period "Winter semester 2023/24" (past)

Time span: 2023-10-01 - 2024-01-28
Selected timetable range:
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Type of class:
Lecture, 10 hours more information
Coordinators: Michał Cyrański
Group instructors: Mihails Arhangelskis, Michał Cyrański
Students list: (inaccessible to you)
Examination: Examination
Course descriptions are protected by copyright.
Copyright by University of Warsaw.
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00-927 Warszawa
tel: +48 22 55 20 000 https://uw.edu.pl/
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