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Sampling and preparation of samples for chromatographic analysis

General data

Course ID:	1200-SPORSchpp
Erasmus code / ISCED:	13.3 Kod klasyfikacyjny przedmiotu składa się z trzech do pięciu cyfr, przy czym trzy pierwsze oznaczają klasyfikację dziedziny wg. Listy kodów dziedzin obowiązującej w programie Socrates/Erasmus, czwarta (dotąd na ogół 0) – ewentualne uszczegółowienie informacji o dyscyplinie, piąta – stopień zaawansowania przedmiotu ustalony na podstawie roku studiów, dla którego przedmiot jest przeznaczony. / (0531) Chemistry The ISCED (International Standard Classification of Education) code has been designed by UNESCO.
Course title:	Sampling and preparation of samples for chromatographic analysis
Name in Polish:	Pobieranie i przygotowanie próbek do analiz chromatograficznych
Organizational unit:	Faculty of Chemistry
Course groups:
ECTS credit allocation (and other scores):	4.00 Basic information on ECTS credits allocation principles: the annual hourly workload of the student’s work required to achieve the expected learning outcomes for a given stage is 1500-1800h, corresponding to 60 ECTS; the student’s weekly hourly workload is 45 h; 1 ECTS point corresponds to 25-30 hours of student work needed to achieve the assumed learning outcomes; weekly student workload necessary to achieve the assumed learning outcomes allows to obtain 1.5 ECTS; work required to pass the course, which has been assigned 3 ECTS, constitutes 10% of the semester student load. view allocation of credits
Language:	Polish
Type of course:	obligatory courses
Short description:	The participant of the study will gain advanced knowledge about the problems of collecting and preparing samples for analysis using chromatographic methods, trace amounts of organic compounds in environmental matrices: water, sewage, air, gases, soil, and others.
Full description:	Sampling and preparation of organic pollutants for determination by chromatographic methods: (I) Air: sampling methods without separating analytes from the matrix, sampling with the use of adsorption, freezing, analytes release methods, etc. (II) Water: sampling, liquid-liquid extraction, liquid-solid extraction (SPE and SPME), liquid-gas extraction. (III) Soil: sampling and preparation, Soxhlet extraction, purification and concentration of extracts. The knowledge gained during the lecture will be supplemented during two laboratory classes: 1. Determination of the index of mineral oil in water, 2. Analysis of volatile air pollutants by extraction method.
Bibliography:	J. Bartulewicz, J. Gawłowski, E. Bartulewicz., Zastosowanie chromatografii gazowej i cieczowej do analizy zanieczyszczeń środowiska, Biblioteka Monitoringu Środowiska, Państwowa Inspekcja Ochrony Środowiska, Warszawa 1997 J. Bartulewicz, J. Gawłowski, E. Bartulewicz., Pobieranie i przygotowanie prób do oznaczania związków organicznych metodami chromatografii, Biblioteka Monitoringu Środowiska, Państwowa Inspekcja Ochrony Środowiska, Warszawa 1997
Learning outcomes:	After completing the course, the participant of the study will understand the advanced problems of environmental sampling and modern methods of sample preparation for the analysis of trace organic pollutants using chromatographic techniques.
Assessment methods and assessment criteria:	Discussion during the lecture, processing of data obtained during work in the laboratory, final exam.

Classes in period "Academic year 2023/24" (in progress)

Time span:	2023-10-01 - 2024-06-16	Selected timetable range: weekly course term Navigate to timetable
Type of class:	Lab, 10 hours more information Lecture, 10 hours more information
Coordinators:	Tomasz Gierczak
Group instructors:	(unknown)
Students list:	(inaccessible to you)
Examination:	Grading

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